共查询到19条相似文献,搜索用时 385 毫秒
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茶皂素提取新工艺研究 总被引:6,自引:0,他引:6
介绍水提法和醇提法从茶饼粕中提取茶皂素的传统工艺,指出茶皂素水解、杂质去除及滤液浓缩是水提法工业化生产茶皂素的三个关键问题。发明了一种新的水提法,浸提前用化学处理抑制、消除茶饼粕中水解酶的活性,有效抑制茶皂素的水解;用纳滤膜浓缩澄清的浸提液,减少废弃相中茶皂素含量;高速离心分离,有效除去浸提液中的糖类、蛋白质、淀粉、果胶等杂质。从2个实例来看:该工艺过程简单、设备投资和生产成本低、能耗少,所得茶皂素产品呈淡黄色,纯度超过80%,得率超过70%。 相似文献
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以油茶饼粕为原料,采用乙醇提取-丙酮沉淀法对茶皂素进行提取分离。以茶皂素纯度和得率为考察指标,对乙醇体积分数、液料比、提取温度、提取时间、提取次数、提取液浓缩程度和丙酮用量等工艺参数进行了单因素优化。结果表明:体积分数95%的乙醇为提取溶剂,乙醇与预处理过的油茶饼粕液料比为9:1(mL:g),提取温度为70℃,提取时间为4 h,提取次数为2次,提取液浓缩至刚好有固体析出,丙酮用量为4倍浓缩液体积量时提取分离效果较佳,得到的茶皂素纯度为85.17%,得率为9.82%。不同溶剂打浆对产品纯化效果的比较发现:丙酮、乙酸乙酯、无水乙醇、体积分数95%的乙醇作为打浆纯化溶剂用于提高茶皂素纯度效果均不明显。 相似文献
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Jun He Zi-ying Wu Shuo Zhang Yang Zhou Feng Zhao Zhi-qin Peng Zhi-wen Hu 《Journal of surfactants and detergents》2014,17(5):919-928
Microwave-assisted extraction (MAE) was utilized to extract tea saponin from oil-tea camellia seed cake. The factors influencing the extraction efficiency were studied, including the effects of microwave power, irradiation duration, temperature, ratio of solvent to material and aqueous ethanol concentration. By systematic orthogonal experiments, the optimal extraction technology was determined. Compared with a conventional extraction method, MAE shows great advantages with the extraction time reduced from 6 h to 4 min, 50 % organic solvent saved and about 14 % extraction yield enhanced. Fourier transform infrared spectroscopy testing and high performance liquid chromatography analysis proved that the extracted resultants were tea saponin with similar compounds as a standard tea saponin. The extracted tea saponin was applied on the cleaning of historic silks and showed good removal effect on the stains. This work provides useful information for fully use of oil-tea camellia seed cake and new applications of tea saponin at the protection of historic textiles. 相似文献
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Wei‐guo Zhang De‐cheng Zhang Xiao‐yuan Chen 《European Journal of Lipid Science and Technology》2012,114(3):352-356
The objective of this study was to extract the oil from Camellia oleifera seed kernels by aqueous enzymatic oil extraction (AEOE). We describe a novel process for extraction of tea oil preceded by tea saponin extraction from C. oleifera seed kernels. The extraction efficiency obtained with microwave‐assisted extraction (MAE) is very high, which the recovery yield is up to 83% in 30 s and the saponins in camellia seed kernels can be completely removed by the second MAE. Moreover, an important step in the process development has been the pretreatment by microwave puffing of camellia seed kernel residues followed by AEOE increased oil extraction yield from 53% to 95%, which will is comparable to hexane oil extraction yields from plant materials. 相似文献
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Jia Xie Tianshun Liu Yingxin Yu Guoxin Song Yaoming Hu 《Journal of the American Oil Chemists' Society》2013,90(5):641-646
Camellia seed oil with high nutritional value is widely used in southern China and southeastern Asia for cooking. Due to the high price of camellia seed oil, fraudulent traders blended the oil with inexpensive oils to increase profits. In this paper, a new method was introduced to detect the adulteration of camellia seed oil with soybean oil by GC–MS with consideration of a parameter which was defined by the total content of oleic and linoleic acid, the oleic to linoleic acid ratio and the content of linolenic acid. Oils samples were prepared by blending pure camellia seed oil with pure soybean oil at levels from 1 to 50 %. Fatty acids esterified by TMSH and TBME in seconds were separated and identified by GC–MS. The detection limit of adulteration was as low as 5 %, and even much lower than 5 % for most kinds of camellia seed oil, which was lower than those measured by other methods. All the results indicated that this simple, accurate and rapid method can also be recommended for the authentication of olive oil with some modification. 相似文献
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从茶籽饼中提取茶皂素的生产工艺研究 总被引:14,自引:0,他引:14
本文就从茶籽饼③中提取茶皂素的生产工艺进行了比较研究,通过对五种不同提取方法的比较,综合了水浸法和有机溶剂法的优点,总结出了一种新的提取工艺──水提──醇萃法。可得到纯度为95%的茶皂素,并且成本低,产率高 相似文献
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茶皂素提取和纯化工艺研究 总被引:1,自引:0,他引:1
以贵州省优势资源油茶利用后产生的油茶籽和废弃茶籽饼为主要原料,从中提取表面活性剂茶皂素,介绍了目前茶皂素的提取和纯化工艺,并进行了一定对比,以对生产实践进行指导。 相似文献
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Junqing Qian Xiaohua Zhao Changyan Zhao Haiyan Yang Lihong Gou Wentao Wang Hui Guo 《European Journal of Lipid Science and Technology》2021,123(1):2000223
High-temperature pretreatment that is currently used in camellia oil extraction can have negative effects on the quality of camellia oil. In this study, the enzymatic pretreatment of camellia seeds is explored as an alternative to high-temperature pretreatment. The main conditions for enzymatic pretreatment of camellia seeds including enzyme, pH, temperature, time, and buffer solution are optimized using the response surface methodology. Under the optimal conditions of enzymatic pretreatment, the oil recovery is close to 75%. Moreover, residual oil recovery from camellia seeds subjected to 1398 neutral protease pretreatment (4 g per kg seeds) and high-temperature pretreatment are 5.62 ± 0.08% and 9.97 ± 0.18%, respectively. The enzymatic pretreatment is further applied to pre-pressing solvent extraction of camellia oil, the cake oil recovery from camellia seeds subjected to enzymatic pretreatment is higher than that from high-temperature pretreatment. These results show that enzymatic pretreatment of camellia seeds has potential for application in the oil industry. Practical Applications : This study suggests that enzymatic pretreatment can replace high-temperature pretreatment and improve oil recovery and oil quality. Ultimately, this method can be used to extract camellia oil. 相似文献
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茶籽皂素的提取及应用研究 总被引:4,自引:0,他引:4
介绍了茶籽皂素在农业、医药、日用化工、养殖、建筑等领域的应用研究,重点综述了近些年从茶籽饼中提取茶皂素的各种提取工艺及其特点,并就茶皂素目前的生产和应用情况提出了一些看法和急需解决的问题。 相似文献