共查询到17条相似文献,搜索用时 625 毫秒
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选用牛骨煅烧的天然羟基磷灰石粉末作为基体,生物活性玻璃为增强相,碳粉为造孔剂,用模压成型法制备多孔羟基磷灰石生物陶瓷。利用XRD进行晶面分析,微孔结构分析仪对试样进行气孔率测试,依据国标对试样进行硬度和抗弯强度的分析,用S-3000N型扫描电镜表征多孔羟基磷灰石生物陶瓷的微观结构。结果表明,随着生物玻璃和碳粉质量百分比的增加,试样组织中的孔隙率的含量和总的孔表面积均随之增加;生物陶瓷的硬度随生物玻璃添加量的增多呈现一定的变化;硬度值较大的试样其抗弯强度都在80MPa,左右,与人体骨相接近;陶瓷微观组织中的孔隙数量和孔径尺寸均随着生物玻璃添加量的增多而增加。 相似文献
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羟基磷灰石生物陶瓷涂层制备方法评述 总被引:19,自引:0,他引:19
根据医用生物陶瓷羟基为磷灰石及医用金属材料的生物,力学特性,本文认为在金属基体表面涂覆羟基磷灰石是综合金属材料及生物陶瓷材料各自优越性阳有希望的途径这一。评述了羟基磷灰石涂层的制备方法,论证了较为优化的涂层结构。 相似文献
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V. V. Shumkova V. M. Pogrebenkov A. V. Karlov V. V. Kozik V. I. Vereshchagin 《Glass and Ceramics》2000,57(9-10):350-353
The results of research and development of bioceramic materials based on calcium hydroxyapatite (HA) and natural mineral wollastonite are reported. The process of production of HA by several reactions is investigated. The optimum bioceramic compositions for medical purposes are determined. 相似文献
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Yu‐Hao Chan Yushan‐Sophie Chang Yun‐Dun Shen Tzu‐Sen Yang Shih‐Fu Ou Ya‐Ju Hsu Mao‐Suan Huang Keng‐Liang Ou 《International Journal of Applied Ceramic Technology》2015,12(1):192-198
A bicalcium phosphate (BCP) bioceramic comprising α‐tricalcium phosphate (α‐TCP) and hydroxyapatite (HA) was prepared by a two‐step sintering. The microstructure of the BCP bioceramic was investigated using scanning electron microscopy (SEM), transmission electron microscopy (TEM), and X‐ray diffraction. The in vitro osteoinductivity was evaluated by culturing MG63 osteoblast‐like cells on the BCP bioceramic. Results showed that the BCP bioceramic comprising α‐TCP and HA in a moderate ratio possessed a hardness of 93.7 Hv. The cells spread faster on the BCP bioceramic than those on the commercial HA. It suggested that the BCP bioceramic can enhance osteoinductivity in vivo. 相似文献
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钛基羟基磷灰石涂层制备技术的研究进展 总被引:7,自引:0,他引:7
钛基HA涂层生物材料作为最有发展前途的生物硬组织替代材料之一,已成为生物医用材料研究的重要内容。本文在综合了大量的国内外文献的基础上,评述了这种涂层主要制备技术的原理、特点及应用。 相似文献
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Sol-Gel Synthesis of Amorphous Calcium Phosphate and Sintering into Microporous Hydroxyapatite Bioceramics 总被引:13,自引:0,他引:13
Pierre Layrolle Atsuo Ito Tetsuya Tateishi 《Journal of the American Ceramic Society》1998,81(6):1421-1428
A new route for preparing hydroxyapatite (Ca10 (PO4 )6 (OH)2 ) bioceramic has been described. An amorphous, nanosized, and carbonate-containing calcium phosphate powder that had a Ca:P ratio of 1.67 was synthesized from calcium diethoxide and phosphoric acid in ethanol via a sol-gel method. The powder was pressed at 98 MPa into green specimens and then heated to a temperature range of 500°-1300°C. At 600°C, the powder crystallized to a carbonated hydroxyapatite and a trace of ß-tricalcium phosphate before converting to hydroxyapatite at 900°C. The thermal crystallization was associated with grain growth, shrinkage, and active surface diffusion. The activation energy of grain growth was 37 ± 2 kJ/mol. After sintering at 1100°C, the decomposition of carbonated hydroxyapatite generated a microporous ceramic with an average pore size of 0.2 µm and an open porosity of 15.5%. This microporous bioceramic can be used as a bone filler. 相似文献
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阐述了国内外学者对金属基羟基磷灰石生物活性涂层的研究状况,论述了羟基磷灰石涂层的制备方法,认为该材料是最具有发展前景的生物硬组织替代材料之一。 相似文献
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To improve the mechanical properties of a porous bioceramic without reducing its porosity, a new kind of porous hydroxyapatite (HA) bioceramic with in-situ grown HA whiskers was fabricated using a simple sintering method. CaSO4·2H2O was used as a pore-forming medium and also as a catalyst for the growth of in-situ HA whiskers. The bioceramic was analyzed by XRD, SEM and mechanical tests. In-situ grown HA whiskers were stratified on the cliffs of pores in the bioceramic. The compressive strength is as high as 21.7 MPa with the porosity of about 26%. The results show that porous HA bioceramic can be improved in both compressive strength and porosity by the addition of CaSO4·2H2O. This novel HA bioceramic has a higher compressive strength without reducing its porosity in a certain weight ratio of CaSO4·2H2O, which depends on its two-step fracture pattern. This novel structure provides a new and promising reinforced pattern for porous materials. 相似文献