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1.
 Mechanical properties and microstructure in high strength hot dip galvanizing TRIP steel were investigated by optical microscope (OM), transmission electron microscope (TEM), X-ray diffraction (XRD), dilatometry and mechanical testing. On the heat treatment process of different intercritical annealing (IA) temperatures, isothermal bainitic transformation (IBT) temperatures and IBT time, this steel shows excellent mechanical properties with tensile strength over 780 MPa and elongation more than 22%. IBT time is a crucial factor in determining the mechanical properties as it confirms the bainite transformation process, as well as the microstructure of the steel. The microstructure of the hot dip galvanizing TRIP steel consisted of ferrite, bainite, retained austenite and martensite during the short IBT time. The contents of ferrite, bainite, retained austenite and martensite with different IBT time were calculated. The results showed that when IBT time increased from 20 to 60 s, the volume of bainite increased from 14.31% to 16.95% and the volume of retained austenite increased from 13.64% to 16.28%; meanwhile, the volume of martensite decreased from 7.18% to 1.89%. Both the transformation induced plasticity of retained austenite and the hardening of martensite are effective, especially, the latter plays a dominant role in the steel containing 7.18% martensite which shows similar strength characteristics as dual-phase steel, but a better elongation. When martensite volume decreases to 1.89%, the steel shows typical mechanical properties of TRIP, as so small amount of martensite has no obvious effect on the mechanical properties.  相似文献   

2.
The effect of additions of Nb, Al and Mo to Fe‐C‐Mn‐Si TRIP steel on the final microstructure and mechanical properties after simulated thermomechanical processing (TMP) has been studied. The laboratory simulations of discontinuous cooling during TMP were performed using a hot rolling mill. All samples were characterised using optical microscopy and image analysis. The volume fraction of retained austenite was ascertained using a heat tinting technique and X‐ray diffraction measurements. Room temperature mechanical properties were determined by a tensile test. From this a comprehensive understanding of the structural aspect of the bainite transformation in these types of TRIP steels has been developed. The results have shown that the final microstructures of thermomechanically processed TRIP steels comprise ~ 50 % of polygonal ferrite, 7 ‐12 % of retained austenite, non‐carbide bainitic structure and martensite. All steels exhibited a good combination of ultimate tensile strength and total elongation. The microstructure‐property examination revealed the relationship between the composition of TRIP steels and their mechanical properties. It has been shown that the addition of Mo to the C‐Si‐Mn‐Nb TRIP steel increases the ultimate tensile strength up to 1020 MPa. The stability of the retained austenite of the Nb‐Mo steel was degraded, which led to a decrease in the elongation (24 %). The results have demonstrated that the addition of Al to C‐Si‐Mn‐Nb steel leads to a good combination of strength (~ 940 MPa) and elongation (~ 30 %) due to the formation of refined acicular ferrite and granular bainite structure with ~7 8 % of stable retained austenite. Furthermore, it has been found that the addition of Al increases the volume fraction of bainitic ferrite laths. The investigations have shown an interesting result that, in the Nb‐Mo‐Al steel, Al has a more pronounced effect on the microstructure in comparison with Mo. It has been found that the bainitic structure of the Nb‐Mo‐Al steel appears to be more granular than in the Nb‐Mo steel. Moreover, the volume fraction of the retained austenite increased (12 %) with decreasing bainitic ferrite content. The results have demonstrated that this steel has the best mechanical properties (1100 MPa and 28 % elongation). It has been concluded that the combined effect of Nb, Mo, and Al addition on the dispersion of the bainite, martensite and retained austenite in the ferrite matrix and the morphology of these phases is different than effect of Nb, Mo and Al, separately.  相似文献   

3.
Multiphase TRIP steels are a relatively new class of steels exhibiting excellent combinations of strength and cold formability, a fact that renders them particularly attractive for automotive applications. The present work reports models regarding the prediction of the stability of retained austenite, the optimisation of the heat‐treatment stages necessary for austenite stabilization in the microstructure, as well as the mechanical behaviour of these steels under deformation. Austenite stability against mechanically‐induced transformation to martensite depends on chemical composition, austenite particle size, strength of the matrix and stress state. The stability of retained austenite is characterized by the MσS temperature, which can be expressed as a function of the aforementioned parameters by an appropriate model presented in this work. Besides stability, the mechanical behaviour of TRIP steels also depends on the amount of retained austenite present in the microstructure. This amount is determined by the combinations of temperature and temporal duration of the heat‐treatment stages undergone by the steel. Maximum amounts of retained austenite require optimisation of the heat‐treatment conditions. A physical model is presented in this work, which is based on the interactions between bainite and austenite during the heat‐treatment of multiphase TRIP steels, and which allows for the selection of treatment conditions leading to the maximization of retained austenite in the final microstructure. Finally, a constitutive micromechanical model is presented, which describes the mechanical behaviour of multiphase TRIP steels under deformation, taking into account the different plastic behaviour of the individual phases, as well as the evolution of the microstructure itself during plastic deformation. This constitutive micromechanical model is subsequently used for the calculation of forming limit diagrams (FLD) for these complex steels, an issue of great practical importance for the optimisation of stretch‐forming and deep‐drawing operations.  相似文献   

4.
Formable high‐strength low‐alloy TRIP‐aided sheet steels with annealed martensite matrix or TRIP‐aided annealed martensitic steel were developed for automotive applications. The steels possessed a large amount of plate‐like retained austenite along annealed martensite lath boundary, the stability of which against the strain‐induced transformation was higher than that of the conventional TRIP‐aided dual‐phase steel with polygonal ferrite matrix. In a tensile strength range between 600 and 1000 MPa, the TRIP‐aided annealed martensitic steels exhibited superior large elongation and reduction of area. In addition, the steels possessed the same excellent stretch‐flangeability and bendability as TRIP‐aided bainitic steel with bainitic ferrite matrix. These properties were discussed by matrix structure, a strength ratio of second phase to matrix, retained austenite stability, internal stress in matrix and so on.  相似文献   

5.
张超  郭辉  王家星  张冰  赵爱民 《工程科学学报》2018,40(12):1502-1509
设计了一种0.7C的低合金超细贝氏体钢,并通过膨胀仪、二体磨损实验、光学显微镜、扫描电镜、X射线衍射、激光扫描共聚焦显微镜及能谱仪,研究了不同等温淬火温度对超细贝氏体钢的贝氏体相变动力学、微观组织以及干滑动摩擦耐磨性的影响,揭示超细贝氏体钢在二体磨损条件下的耐磨性能和磨损机理.研究结果表明,不同等温温度下的超细贝氏体钢都由片层状贝氏体铁素体和薄膜状以及块状的残留奥氏体组成;随着等温温度的升高,超细贝氏体的相变速率提高,相变孕育期及相变完成时间缩短,但贝氏体铁素体板条厚度增加,残留奥氏体含量增加,硬度值有所降低;超细贝氏体钢磨损面形貌以平直的犁沟为主,主要的磨损机理为显微切削;不同等温温度下所获得的超细贝氏体的耐磨性能都优于回火马氏体,且随着等温温度的降低,耐磨性能提高.其中在250℃等温所获得的超细贝氏体钢具有最优的耐磨性能,其相对耐磨性为回火马氏体的1.28倍.这主要与超细贝氏体钢中贝氏体铁素体板条的细化及磨损过程中残留奥氏体的形变诱导马氏体相变(TRIP)效应有关.   相似文献   

6.
Retained austenite as a key constituent in final microstructure plays an important role in TRansformation Induced Plasticity (TRIP) steels. The volume fraction, carbon concentration, size, and morphology of this phase are the well‐known parameters which effects on the rate of transformation of retained austenite to martensite and the properties of steel, are studied by many researchers. Of the transformation of retained austenite to martensite under strain in a TRIP steel is studied in this paper. The experimental results show that the transformation rate of retained, austenite with similar characteristics, to martensite in differently processed TRIP steel samples, exhibits an anisotropic behavior. This phenomenon implies a kind of variant selection of martensitic reaction of retained austenite under strain and is explained by ferrite texture developed in steel.  相似文献   

7.
Multiphase TRIP steels exhibit unique combinations of strength and cold formability, characteristics especially desirable in automotive applications. This behaviour is largely determined by the amount and stability of the retained austenite dispersion in the microstructure, produced by a two‐stage heat‐treatment, consisting of intercritical annealing followed by an isothermal bainitic treatment. The amount and stability of retained austenite is mainly determined by the proper selection of the temperature and temporal duration of the bainitic treatment. In the present work an approach is presented which allows for the calculation of the amount of retained austenite in the microstructure, as a function of bainitic treatment conditions. The approach is based on the physical characteristics of the bainitic transformation and on the stabilizing effects of the formation of bainitic ferrite in austenite. Each bainitic ferrite platelet is considered to chemically stabilize a part of the surrounding austenite due to carbon rejection. The spatial and temporal extent of this stabilization is determined by solving the corresponding carbon‐diffusion problem, and thus the amount of retained austenite contributed by any individual platelet is determined. Subsequently, the evolution of the population of the platelets in the entire microstructure is determined and, thus, the volume fraction of retained austenite as a function of transformation time is calculated. Application and comparison of calculations with experimental results, obtained from four different multiphase TRIP steel compositions, exhibited very good qualitative and quantitative agreement.  相似文献   

8.
Designing of alloy concept and process for DP,TRIP and TWIP steels stressing at martensite transformation are analyzed.For DP steel,austenite volume percent and its carbon content at different intercritical temperatures are calculated as well as the tensile strength of the steel,which meet well with the experimental result.The condition for dissolution of carbide is discussed by experiments and predicted by kinetic estimation.Several sample TRIP steels are prepared and their concentration profiles are calculated showing different diffusion characteristics of elements.Calculation also shows carbon enrichment is successful in this stage through the quick diffusion of carbon from ferrite to austenie.In order to maintain the austenite stability or to prevent precipitation of cementite,minimum cooling rate from the intercritical zone to over aging stage is obtained through kinetic simulation.Bainite transformation is estimated,which indicates the carbon rerichment from ferrite of bainite structure to austenite in this stage is also successful.Thermal HCP martensite transformation and the strain induced martensite transformation in TWIP steel is introduced.Relationship between transformation and mechanical properties in the steel is also mentioned.  相似文献   

9.
Steels with compositions that are hot rolled and cooled to exhibit high strength and good toughness often require a bainitic microstructure. This is especially true for plate steels for linepipe applications where strengths in excess of 690 MPa (100 ksi) are needed in thicknesses between approximately 6 and 30 mm. To ensure adequate strength and toughness, the steels should have adequate hardenability (C. E. >0.50 and Pcm >0.20), and are thermomechanically controlled processed, i.e., controlled rolled, followed by interrupted direct quenching to below the Bs temperature of the pancaked austenite. Bainite formed in this way can be defined as a polyphase mixture comprised a matrix phase of bainitic ferrite plus a higher carbon second phase or micro-constituent which can be martensite, retained austenite, or cementite, depending on circumstances. This second feature is predominately martensite in IDQ steels. Unlike pearlite, where the ferrite and cementite form cooperatively at the same moving interface, the bainitic ferrite and MA form in sequence with falling temperature below the Bs temperature or with increasing isothermal holding time. Several studies have found that the mechanical properties may vary strongly for different types of bainite, i.e., different forms of bainitic ferrite and/or MA. Thermomechanical controlled processing (TMCP) has been shown to be an important way to control the microstructure and mechanical properties in low carbon, high strength steel. This is especially true in the case of bainite formation, where the complexity of the austenite-bainite transformation makes its control through disciplined processing especially important. In this study, a low carbon, high manganese steel containing niobium was investigated to better understand the effects of austenite conditioning and cooling rates on the bainitic phase transformation, i.e., the formation of bainitic ferrite plus MA. Specimens were compared after transformation from recrystallized, equiaxed austenite to deformed, pancaked austenite, which were followed by seven different cooling rates ranging between 0.5 K/s (0.5 °C/s) and 40 K/s (40 °C/s). The CCT curves showed that the transformation behaviors and temperatures varied with starting austenite microstructure and cooling rate, resulting in different final microstructures. The EBSD results and the thermodynamics and kinetics analyses show that in low carbon bainite, the nucleation rate is the key factor that affects the bainitic ferrite morphology, size, and orientation. However, the growth of bainite is also quite important since the bainitic ferrite laths apparently can coalesce or coarsen into larger units with slower cooling rates or longer isothermal holding time, causing a deterioration in toughness. This paper reviews the formation of bainite in this steel and describes and rationalizes the final microstructures observed, both in terms of not only formation but also for the expected influence on mechanical properties.  相似文献   

10.
Recently various kinds of high-strength sheet steels have been developed to meet the requirements of the automotive industry such as passive safety, weight reduction and saving energy. Usually the main problem of high-strength steels is their inferior ductility. Multiphase steels however show a very good combination of strength and formability so that the applicable region of high-strength steels has been widely enlarged. Multiphase steels have been developed for various purposes because of their ability to tailor properties by adjusting the type, the amount, and the distribution of different phases. Especially new developed triple-phase steels which make use of the TRIP effect (transformation induced plasticity) can further improve formability as well as strength due to the transformation of retained austenite to martensite during the deformation. In this work the transformation behaviour and the mechanical properties of low alloyed TRIP steels were investigated. The influence of the annealing parameters on transformation behaviour and on the amount of retained austenite were determined. In addition the temperature dependence of the mechanical properties and the effect of testing speed on the formability were studied. The investigation was carried out on seven different TRIP steels with different chemical compositions, especially the influence of the microalloying element niobium was considered. For reasons of comparison various mild and high-strength steels were tested parallel to the TRIP steels. It was found that the investigated TRIP steels offer very attractive combinations of elongation and strength values. An interesting temperature dependence of the mechanical properties can be observed, in such a way that the elongation values of the TRIP steels possess a maximum between +50 and +100°C. Due to its effect on grain size and on precipitation behaviour the addition of niobium leads to higher strength values without a strong decrease in ductility. In general, the mechanical properties are strongly affected by the type and the distribution of the different phases. The most important parameters, however, to influence the mechanical behaviour are the amount and the stability of the retained austenite, which are mainly controlled by the heat treatment and the chemical composition.  相似文献   

11.
The transformation, microstructure and mechanical properties of the 0. 2C- 5Mn TRIP steel after intercritical annealing were investigated using dilatometer, scanning electronic microscopy (SEM), transmission electron microscopy(TEM), X- ray diffraction (XRD), and tensile testing machine. The phase transformation thermodynamics of the investigated steel after intercritical annealing was calculated by Factsage software and the characteristics of the transformation were discussed. The results show that the reversed austenite content increases with the increasing of the intercritical annealing temperature, the carbon content in reversed austenite firstly increases and then decreases, manganese content in reversed austenite decreases, which results in the decreasing of the thermal stability of reversed austenite. When the intercritical annealing temperature is 700??, an obvious martensitic transformation occurs during the cooling process. With the increasing of intercritical annealing temperature, cementite is gradually dissolved, but it cannot be completely dissolved due to the short transformation time. When the intercritical annealing temperature is 600-675??, the microstructure after intercritical annealing consists of ferrite, cementite and retained austenite. When the intercritical annealing temperature is 700??, the microstructure after intercritical annealing consists of ferrite, retained austenite, martensite and a small amount of undissolved cementite. The engineering stress and strain curves of the investigated steel are significantly changed with increasing intercritical annealing temperature. At the same time, the optimal mechanical properties with tensile strength of 1138MPa and total elongation of 23% can be obtained after annealed at 675?? for 3min.  相似文献   

12.
Dual-phase and transformation-induced plasticity (TRIP)-assisted multiphase steels are related families of high-strength formable steels exhibiting excellent mechanical characteristics. This study shows how a ferrite-bainite-martensite microstructure containing retained austenite can improve the mechanical properties of a cold-rolled low-carbon, low-silicon steel. Such a multiphased microstructure is obtained by a heat treatment involving intercritical annealing followed by a bainite transformation tempering. Depending on the heat-treatment parameters, the samples present a variety of microstructures. Due to the presence of retained austenite, some samples exhibit a TRIP effect not anticipated with such a low silicon content. A composite strengthening effect also results from the simultaneous presence of a ductile ferrite matrix with bainite and martensite as hard second phases. A true stress at maximum load of 800 MPa and a true uniform strain of 0.18 can be obtained by forming a ferrite-bainite-martensite microstructure containing up to 10 pct of retained austenite. These properties correspond to a favorable evolution of work hardening during plastic deformation.  相似文献   

13.
The stability of retained austenite and the kinetics of the strain‐induced martensitic transformation in micro‐alloyed TRIP‐aided steel were obtained from interrupted tensile tests and saturation magnetization measurements. Tensile tests with single specimens and at variable temperature were carried out to determine the influence of the micro‐alloying on the Msσ temperature of the retained austenite. Although model calculations show that the addition of the micro‐alloying elements influences a number of stabilizing factors, the results indicate that the stability of retained austenite in the micro‐alloyed TRIP‐aided steels is not significantly influenced by the micro‐alloying. The kinetics of the strain‐induced martensitic transformation was also not significantly influenced by addition of the micro‐alloying elements. The addition of micro‐alloying elements slows down the autocatalytic propagation of the strain‐induced martensite due to the increase of the yield strength of retained austenite. The lower uniform elongation of micro‐alloyed TRIP‐aided steel is very likely due to the presence of numerous precipitates in the microstructure and the pronounced ferrite grain size refinement.  相似文献   

14.
通过Gleeble-1500热模拟压缩试验,借助光学显微镜、扫描电镜、X射线衍射及拉伸试验等,研究一种低碳Mn-Si钢在基于热轧动态相变的热轧TRIP钢工艺和基于贝氏体等温处理工艺下的组织与力学性能,比较了通过两种工艺获得的不同复相组织状态对材料的加工硬化能力的影响.结果表明:实验钢在基于动态相变的热轧TRIP钢工艺下获得了以细晶铁素体为基体和贝氏体、残余奥氏体组成的复相组织,而在基于贝氏体等温处理工艺下得到了以板条贝氏体为基体和残余奥氏体组成的复相组织,前者中残余奥氏体含量较高且其碳含量也较高.实验钢具有以板条贝氏体为基体的复相组织时屈服强度和抗拉强度较高;但由于残余奥氏体稳定性较差,实验钢的加工硬化能力较弱,导致其均匀延伸率和总延伸率较小.   相似文献   

15.
Herein, the microstructure and mechanical properties of a high-carbon bainitic steel treated by long-time bainitic austempering and short-time austempering plus tempering processes are compared. The multiphase microstructures are characterized by dilatometry, X-ray diffraction, scanning electron microscopy, and transmission electron microscopy to correlate with mechanical properties. Results show that although long-time austempering treatment can reduce the volume fraction of brittle martensite, no significant improvement is observed in fracture damage resistance. Besides, the cementite is prone to precipitation from the austenite at the later period of the long-time austempering process. The cementite precipitation in austenite decreases the carbon content in retained austenite (RA) and consequently reduces the mechanical stability of RA. In contrast, the cementite has not been able to precipitate from austenite after short-time austempering treatment, whereas the martensite is softened and the stability of RA is improved during subsequent tempering. Therefore, excellent mechanical properties are obtained in the samples treated by short-time austempering plus tempering process: ultimate tensile strength, 1489 MPa, yield strength, 1014 MPa, total elongation, 33.2%, and the product of strength and elongation (PSE) of 48.4 GPa%, where PSE is increased by 27% compared with the sample after long-time bainitic austempering.  相似文献   

16.
利用扫描电子显微镜(SEM)、透射电子显微镜(TEM)、电子探针(EPMA)、X射线衍射仪(XRD)、室温拉伸等手段, 通过两相区保温-淬火(IQ)、两相区形变后保温-淬火(DIQ)、两相区保温-淬火-配分-贝氏体区等温(IQ&PB)及两相区形变后保温-淬火-配分-贝氏体区等温(DIQ&PB)热处理工艺, 研究高温形变对室温组织、性能、残余奥氏体稳定性的综合影响作用.结果表明, 经15%的压缩形变后铁素体中位错密度由0.290×1014增加至1.286×1014 m-2, 马氏体(原奥氏体)中C、Cu元素富集浓度提高, 高温形变产生位错增殖对元素配分有明显促进作用.DIQ&PB工艺下, 形变后贝氏体板条尺寸变短且宽度增加0.1 μm左右, 贝氏体转变量较未变形时增加14%, 多边形铁素体尺寸明显减小.力学性能方面, 两相区形变热处理后抗拉强度增加132.85 MPa, 断后伸长率增加7%, 强塑积可达25435 MPa·%.形变后残余奥氏体体积分数由7.8%提高到8.99%, 残余奥氏体中碳质量分数由1.05%提高到1.31%.   相似文献   

17.
By using a static and high-speed material testing machine,tensile deformation behaviors of two kinds of SiMn TRIP(transformation induced plasticity)steels and DP(dual phase)steel were studied in a large range of strain rates(0.001-2 000s-1).Temperature variation during adiabatic heating and the amount of retained austenite at fracture were measured by an infrared thermometer and an X-ray stress analyser,respectively.The microstructure of steels was observed by optical microscopy(OM)and scanning electron microscopy(SEM)before and after tensile test.It was found from the experimental results that the tensile strength of these steels increased,and the fracture elongation firstly decreased and subsequently increased,as the strain rate increased in the range of 0.1-2 000s-1.The temperature raised during adiabatic heating of TRIP steel was in the range of 100-300℃,while that of the DP steel was in the range of 100-220 ℃.The temperature rise of these steels increased with increasing the strain rate,as well as the amount of the transformed retained austenite in TRIP steels.It was confirmed that austenite to martensite transformation is not suppressed by adiabatic heating.  相似文献   

18.
Low-alloy multiphase transformation-induced-plasticity (TRIP) steels offer excellent mechanical properties in terms of elongation and strength. This results from the complex synergy between the different phases, i.e., ferrite, bainite, and retained austenite. The precise knowledge of the austenite-to-martensite transformation kinetics is required to understand the behavior of TRIP steels in a wide array of applications. The parameters determining the stability of the metastable austenite were reviewed and investigated experimentally, with special attention paid to the effect of the chemical composition, the temperature, and the size of the austenite particles. The results show that the stability and rate of transformation of the austenite particles in TRIP steels have a pronounced composition dependence: austenite particles transform at a faster rate in CMnSi TRIP steel than in TRIP steels in which Si is fully or partially replaced by Al and P. The results clearly support the view that (1) both a high C content and a submicron size are required for the room-temperature stability of the austenite particles and (2) the effect of the chemical composition on the transformation is due to its influence on the intrinsic stacking-fault energy. In addition, the composition dependence of the Md 30 temperature was derived by regression analysis of experimental data. The influence of the size of the retained austenite particles on their Ms σ temperature was studied by means of a thermodynamic model. Both the analysis of the transformation-kinetics data and the microstructural analysis by transmission electron microscopy revealed the very limited role of autocatalysis in the transformation.  相似文献   

19.
Austempering of Hot Rolled SiMn TRIP Steels   总被引:2,自引:1,他引:1  
 The austempering after hot rolling in hot rolled Si Mn TRIP (transformation induced plasticity) steels was investigated. The mechanism of TRIP was discussed through examination of the microstructure and the mechanical properties of this kind of steel. The results showed that the strain induced transformation to martensite of retained austenite occurs in hot rolled Si Mn TRIP steels. The sample exhibited a good combination of ultimate tensile strength and total elongation when it was held at the bainite transformation temperature after hot deformation. The stability of retained austenite increases with an increase in isothermal holding time, and a further increase in the holding duration resulted in the decrease of stability. The mechanical properties were optimal when holding for 25 min, and tensile strength and total elongation reached the maximum values (774 MPa and 33%, respectively).  相似文献   

20.
Advanced high‐strength steels, like dual phase and TRIP steels, have gained much interest for automotive application. The complex microstructures in dual phase steels, and even more critical, the metastable microstructure in TRIP steels, do not follow the well‐established traditional microstructure‐property relationships for deep drawing steels. The volume fraction of the different phases, the phase distribution, and the stability of metastable phases influence significantly the forming potential. This paper discusses the correlation between different microstructural features and the mechanical properties. The tensile test properties of dual phase steels are governed by the martensite volume fraction, the martensite hardness and to a much smaller extent the martensite island diameter. Both in dual phase and more pronounced in TRIP steels the retained austenite content plays a vital role in determining the formability. The stability of the retained austenite can be described by different methods, it needs to be adjusted according to the forming temperature and the type and amount of strain. In general, multiphase steels require a very strict microstructure control in order to develop predictable forming behaviour.  相似文献   

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