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1.
唑螨酯在苹果和柑桔上的残留动态   总被引:3,自引:0,他引:3  
平霄飞  吴园生 《农药》1994,33(6):24-25,23
本文报道了唑螨酯在苹果、柑桔及土壤中的降解动态和最终残留状况。结果表明,唑螨酯在苹果全果和桔皮中,施药后1周内降解较快,之后缓慢;在土壤中降解较慢。半衰期分别为苹果6.0天,桔皮19.7天,土壤51天。收获时的安全间隔期为20~47天。苹果全果、桔皮和桔肉中的最终残留量均有检出,但含量较低,苹果和桔肉中最高为0.09毫克/公斤,桔皮中小于0.2毫克/公斤。  相似文献   

2.
王洪涛  许志强 《农药》1997,36(8):30-32
本文概述了涕灭威及其代谢物在苹果和土壤中残留量的分析方法。样品以内酮提取,过氧乙酸氧化,二氯甲烷萃取,气火焰光度检测器测定。涕灭威在土壤和苹果中的最低检测浓度分别为0.004、0.004毫克/公斤,空白样品添加0.1-2.0毫克/公斤,涕灭威及其代谢物的平均回收率和变异系数分别为84.7-109.7%及1.0-7.8%。  相似文献   

3.
腈菌唑在小麦,土壤上残留与降解的动态试验研究   总被引:1,自引:2,他引:1  
夏昕  吴剑英 《农药》1996,35(10):29-31
本试验为腈菌唑在辽宁、江苏两地的两年残留测定,作物为小麦。分析目标为麦粉、麦杆、青植株、土壤,四种试材分析方法的添加回收率均为75%以上。1993年土壤的半衰期辽宁、江苏分别为27.2天和23.7天,小麦青植株的半衰期辽宁、江苏分别为2.1天和2.5天;1994年土壤的半衰期辽宁、江苏分别为25.8天和36.7天,小麦青植株的半衰期辽宁、江苏分别为4.3天和3.3天。试验施药剂量为25毫克/公斤(2.5克/亩)及50毫克/公斤(5.0克/亩)两种,在收获期小麦麦粉及麦杆中的残留量都低于参照的允许残留量0.1毫克/公斤及2.0毫克/公斤,安全间隔期为20天。分析结果表明腈菌唑对小麦使用安全。  相似文献   

4.
黄士忠  李治祥 《农药》1996,35(6):30-31
本文概述了酰胺唑及其代谢物在土壤和梨中残留量的分析方法,样品以丙酮提取,二氯甲烷萃取,氟罗里硅土柱净化,气谱电子捕获检测器测定。IM和IBC-01的最小检测量为8.1×10^-11克,5.0×10^-11克,在土壤和梨中的最低检测浓度分别为0.0089、0.0067毫克/公斤和0.0056,0.0042毫克/公斤。  相似文献   

5.
本文概述了涕灭威及其代谢物在苹果和土壤中残留量的分析方法。样品以丙酮提取,过氧乙酸氧化,二氯甲烷萃取,气谱火焰光度检测器(GC/FPD)测定。涕灭威在土壤和苹果中的最低检测浓度分别为0004、0004毫克/公斤,空白样品添加01~20毫克/公斤,涕灭威及其代谢物的平均回收率和变异系数分别为847~1097%及10~78%。  相似文献   

6.
苯黄隆在小麦和土壤中的残留研究   总被引:2,自引:0,他引:2  
经高效液相色谱法测定,最小检知量为1×10 ̄-9克,麦面中最低检知浓度为0.05毫克/公斤,土壤中为0.025毫克/公斤。麦面中回收率为75.5~79.8%,变异系数为3.53~5.94%;土壤中回收率为101.0~106.2%,变异系数为4.43~6.16%。  相似文献   

7.
胡莲英  赵华 《农药》1994,33(5):36-37,28
本文主要研究喹禾灵在花生植株及土壤环境中的残留与降解动态,采用气相色谱法电子捕获检定器(ECD)测定。仪器的最小检出量为1×10 ̄(-11)克,样品的最低检出浓度为0.001毫克/千克。喹禾灵本体在花生叶、花生仁、土壤中的平均回收率分别为:82.1~83.3%、82.9~86.1%、83.6~92.3%,变异系数依次为2.7~8.7%、3.2~5.3%、0.8~6.2%;喹禾灵酸在花生仁和土壤中的平均回收率分别为85.2~88.4%、81.7~88.4%,变异系数依次为3.9~5.8%、6.7~7.8%。  相似文献   

8.
气相色谱法测定玉米中乙草胺残留量   总被引:2,自引:0,他引:2  
俞苏霞  蒋世熙 《农药》1997,36(12):26-27
本文报道了玉米中乙草胺残留量的气相色谱测定法,样品用石油醚-丙酮提取,乙腈液-液分配净化,电子捕获检测器测定。乙草胺的最小检测量为8.6×10^-12克,在玉米中最低检测浓度0.001毫克/公斤。空白样品添加0.04-1.00毫克/公斤的平均回收率和变异系数分别为94.5%和2.6%。  相似文献   

9.
王强 《农药》1995,34(2):15-17
作者以柑桔全爪螨为供试材料,对杀螨剂-哒螨灵和唑螨酯的室内毒力,杀螨杀卵活性,毒杀作用特点及田间效等进行研究,结果表明,哒螨灵对雌成螨和卵均具有极高的毒力(LC50分别为0.21和0.12ppm),其相对毒力指数均居供试六种杀螨剂之首位,唑螨酯对雌成螨也具有较高的毒力(LC50为0.94ppm),其相对毒务指数也高于苯丁锡,噻螨酮,三唑锡及克螨特,但唑螨酯对卵的毒力(LC50 20.5ppm)则低于噻螨酮,同时,哒螨灵0.75-1ppm和唑螨酯2-10ppm的杀螨活性均达90%以上,哒螨灵0.2-0.75ppm的杀卵活性也达80%以上,而唑螨酯50ppm的杀卵活性则为60.7%,二者不仅击倒作用迅速,如唑螨酯5和50ppm的击倒中时分别为19.53和7.71小时,而且持效期长,田间小区试验表明,15%哒螨灵乳油30000-4000倍和5%唑螨酯悬浮剂1000-2000倍防治柑桔全爪螨有较好效果,药后3天即可见效,药效可分别维持40天和30天。  相似文献   

10.
以7%聚丙二醇己二酸酯/ChromosorbG,AWDMCS为填充柱,以苯酚为内标物,在适宜的色谱条件下对2-溴-2-溴甲基戊二腈进行了定量分析。变异系数0.17%;回收率98。90~101.2%。  相似文献   

11.
Scentless plant bugs (Heteroptera: Rhopalidae) are so named because adults of the Serinethinae have vestigial metathoracic scent glands. Serinethines are seed predators of Sapindales, especially Sapindaceae that produce toxic cyanolipids. In two serinethine species whose ranges extend into the southern United States,Jadera haematoloma andJ. sanguinolenta, sequestration of host cyanolipids as glucosides renders these gregarious, aposematic insects unpalatable to a variety of predators. The blood glucoside profile and cyanogenesis ofJadera varies depending on the cyanolipid chemistry of hosts, and adults and larvae fed golden rain tree seeds (Koelreuteria paniculata) excrete the volatile lactone, 4-methyl-2(5H)-furanone, to which they are attracted.Jadera fed balloon vine seeds (Cardiospermum spp.) do not excrete the attractive lactone. Loss of the usual heteropteran defensive glands in serinethines may have coevolved with host specificity on toxic plants, and the orientation ofJadera to a volatile excretory product could be an adaptive response to save time.Mention of a commercial product does not consititute an endorsement by the USDA.  相似文献   

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Vismiones and ferruginins, representatives of a new class of lypophilic anthranoids from the genusVismia were found to inhibit feeding in larvae of species ofSpodoptera, Heliothis, and inLocusta migratoria.  相似文献   

14.
2008~2009年世界塑料工业进展   总被引:4,自引:1,他引:3  
收集了2008年7月~2009年6月世界塑料工业的相关资料,介绍了2008~2009年国外塑料工业的发展情况,提供了世界塑料产量、消费量及全球各类树脂的需求量及产能情况。按通用热塑性树脂(聚乙烯、聚丙烯、聚苯乙烯、聚氯乙烯、ABS树脂)、工程塑料(尼龙、聚碳酸酯、聚甲醛、热塑性聚酯、聚苯醚)、特种工程塑料(聚苯硫醚、液晶聚合物、聚醚醚酮)、通用热固性树脂(酚醛、聚氨酯、环氧树脂、不饱和聚酯树脂)不同品种的顺序,对树脂的产量、消费量、供需状况及合成工艺、产品应用开发、树脂品种的延伸及应用的进一步扩展等技术作了详细介绍。  相似文献   

15.
It is well established that a wide range of drugs of abuse acutely boost the signaling of the sympathetic nervous system and the hypothalamic–pituitary–adrenal (HPA) axis, where norepinephrine and epinephrine are major output molecules. This stimulatory effect is accompanied by such symptoms as elevated heart rate and blood pressure, more rapid breathing, increased body temperature and sweating, and pupillary dilation, as well as the intoxicating or euphoric subjective properties of the drug. While many drugs of abuse are thought to achieve their intoxicating effects by modulating the monoaminergic neurotransmitter systems (i.e., serotonin, norepinephrine, dopamine) by binding to these receptors or otherwise affecting their synaptic signaling, this paper puts forth the hypothesis that many of these drugs are actually acutely converted to catecholamines (dopamine, norepinephrine, epinephrine) in vivo, in addition to transformation to their known metabolites. In this manner, a range of stimulants, opioids, and psychedelics (as well as alcohol) may partially achieve their intoxicating properties, as well as side effects, due to this putative transformation to catecholamines. If this hypothesis is correct, it would alter our understanding of the basic biosynthetic pathways for generating these important signaling molecules, while also modifying our view of the neural substrates underlying substance abuse and dependence, including psychological stress-induced relapse. Importantly, there is a direct way to test the overarching hypothesis: administer (either centrally or peripherally) stable isotope versions of these drugs to model organisms such as rodents (or even to humans) and then use liquid chromatography-mass spectrometry to determine if the labeled drug is converted to labeled catecholamines in brain, blood plasma, or urine samples.  相似文献   

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Halyomorpha halys (Stål) (Pentatomidae), called the brown marmorated stink bug (BMSB), is a newly invasive species in the eastern USA that is rapidly spreading from the original point of establishment in Allentown, PA. In its native range, the BMSB is reportedly attracted to methyl (E,E,Z)-2,4,6-decatrienoate, the male-produced pheromone of another pentatomid common in eastern Asia, Plautia stali Scott. In North America, Thyanta spp. are the only pentatomids known to produce methyl 2,4,6-decatrienoate [the (E,Z,Z)-isomer] as part of their pheromones. Methyl 2,4,6-decatrienoates were field-tested in Maryland to monitor the spread of the BMSB and to explore the possibility that Thyanta spp. are an alternate host for parasitic tachinid flies that use stink bug pheromones as host-finding kairomones. Here we report the first captures of adult and nymph BMSBs in traps baited with methyl (E,E,Z)-2,4,6-decatrienoate in central Maryland and present data verifying that the tachinid, Euclytia flava (Townsend), exploits methyl (E,Z,Z)-2,4,6-decatrienoate as a kairomone. We also report the unexpected finding that various isomers of methyl 2,4,6-decatrienoate attract Acrosternum hilare (Say), although this bug apparently does not produce methyl decatrienoates. Other stink bugs and tachinids native to North America were also attracted to methyl 2,4,6-decatrienoates. These data indicate there are Heteroptera in North America in addition to Thyanta spp. that probably use methyl 2,4,6-decatrienoates as pheromones. The evidence that some pentatomids exploit the pheromones of other true bugs as kairomones to find food or to congregate as a passive defense against tachinid parasitism is discussed.  相似文献   

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