LED显示屏用有机硅灌封胶的研制

制备了一种LED显示屏用有机硅灌封胶。研究不同粉体对胶黏附性、抗沉淀性的影响,不同厂家生产的3号白油及其含量对耐低温性的影响,不同偶联剂对深层固化的影响。配方优化后制备的胶深层固化好,不粘灯,放置3个月粉体不沉淀,在-30℃下固化后的胶体表面无油渗出。     

电气电子灌封在电力电子设备中的应用及实现

对电子元器件进行灌封，需要对电子元器件进行科学合理的布置、组装、连接与保护等工艺操作，具有较好的抵抗外部冲击力和防水、防潮和防腐蚀性能，不同电子元件和线路间的绝缘性能也可以得到优化，可以提升器件整体性。本文先对环氧树脂、聚氨酯和有机硅3种灌封材料进行分析与研究，并进行性能对比分析，再对市面上主流的电路板灌封胶进行分析和选型，对PCBA板灌封工艺研究，最后就灌封质量问题提出解决办法，可供相关人员参考。     

室温快速固化高性能环氧树脂胶粘剂研究

为了提高胶粘剂在室温条件下的固化速度,并改善其力学性能,研究了固化剂含量、填料含量对环氧树脂胶粘剂固化速度和力学性能的影响.结果表明,当固化剂含量为95～100 phr,填料含量为60～ 80 phr时,胶粘剂的综合性能最好;该新型胶粘剂在室温12 min即可快速固化,剪切强度可达13.8 MPa,拉伸强度和弯曲强度分别达到了43.1MPa和83.2 MPa.     

T700和T300碳纤维增强环氧树脂基复合材料耐湿热老化性能的对比

在温度为70℃、相对湿度为85%的湿热环境下,分别对T700碳纤维/环氧树脂基复合材料、T300碳纤维/环氧树脂基复合材料以及两种复合材料/金属胶接结构进行了70 d的加速老化试验,并对老化前后的试样进行了力学性能试验和无损检测.结果表明:湿热环境没有改变两种复合材料的破坏模式,但使复合材料的纵、横向压缩强度和剪切强度略有降低;对复合材料/金属胶接结构,湿热老化环境不会导致胶接界面产生损伤,但会使胶接强度下降;老化前两种复合材料的力学性能基本相当,老化70 d后T700碳纤维/环氧树脂基复合材料的性能保持率略优.     

室温固化方舱大板结构胶的研制

本文采用聚氨酯增韧改性环氧树脂配制一种室温固化方舱大板结构胶。通过红外光谱测试、扫描电镜分析,得知此种大板结构胶有较好的稳定性和较好的韧性;通过剪切强度、剥离强度测试,得知该胶有较高的力学性能;同时该胶也有很好的耐介质性能。     

电子工业防潮浇注密封材料——DO4透明硅橡胶浇注-胶粘剂

电子工业的迅速发展,需大量采用防潮浇注材料。例如在电子元件的结合处,为达到防潮避振目的,经常采用透明的所谓针入复元的透明性凝胶体进行灌封,在不少场合(例如在印刷电路板上)要求灌封料固化后具有较高的物理机械性能,因而采用了室温固化硅橡胶浇注料。     

三胶筒封隔器胶筒的密封性能分析

以三胶筒封隔器为研究对象,应用ANSYS有限元软件建立了封隔器密封元件的计算模型,分析了不同坐封载荷下胶筒的变形、胶筒与套管接触压力的变化规律。计算结果表明,弹性模量相对较小的中胶筒首先与套管接触,其次是靠近载荷施加端的胶筒与套管接触,远离载荷施加端的胶筒最后与套管接触。三段胶筒与套管的接触压力都随坐封载荷的增大而增大,在不同坐封载荷下,靠近载荷施加端的胶筒与套管的接触压力均大于中间胶筒和远离载荷施加端胶筒的压力,靠近载荷施加端的胶筒与套管的接触压力越大,封隔器的密封性能越好。     

酚醛树脂/石墨模压成型复合材料双极板的制备与性能

以石墨与酚醛树脂粉料为原料通过低温热模压成形工艺制备低成本酚醛树脂／石墨复合材料双极板，对材料的力学性能与导电性能进行了研究。结果表明：酚醛树脂含量是影响复合材料导电性能与力学性能的主要因素，酚醛树脂含量低于20％时，材料具有较高的导电性能；提高固化温度与固化压力，可以提高材料的抗弯强度，但材料的导电性能明显降低；适中的固化压力与固化温度有利于材料具有较好的力学性能与导电性能。     

快速凝固结合粉末冶金法制备SiC_p/AZ91复合材料的组织及性能

用快速凝固结合粉末冶金法制备了SiC颗粒增强镁合金基复合材料(SiCp/AZ91)棒材,研究了SiC颗粒含量对复合材料室温力学性能及显微组织的影响.结果表明:制备的复合材料棒材中SiC颗粒在基体中分布均匀,但仍存在局部颗粒团聚现象;随SiC颗粒含量的增加,复合材料的屈服强度、抗拉强度和断后伸长率均逐渐降低;热挤压过程中,镁、SiC和SiO2之间发生了界面反应,在界面生成Mg2Si等脆性相,影响了复合材料的界面性能.     

c-BN增强(Ti,W)C基复合金属陶瓷刀具材料的研制

采用热压烧结制备了不同亚微米级c-BN含量的(Ti,W)C基复合金属陶瓷刀具材料,用热场发射扫描电子显微镜及能谱仪、透射电子显微镜和X射线衍射仪对材料的微观组织结构和力学性能进行了研究。结果表明:添加c-BN可改善材料的力学性能,当c-BN含量为1.5wt%时,(Ti,W)C基复合金属陶瓷刀具的性能最优,其抗弯强度达到917MPa,断裂韧性为9.27MPa·m~(1/2),维氏硬度为20.64GPa;适量c-BN可起到细化晶粒、减少气孔缺陷和提高致密度的作用,复合材料由沿晶断裂为主转变为穿晶断裂为主;在c-BN复合(W,Ti)C基金属陶瓷刀具材料中,主要的增韧补强机理有晶粒细化、颗粒桥联、裂纹偏转和裂纹分叉。     

导热硅胶垫选型和性能探究

通过不同加强材料下导热硅胶垫性能的比对,不同导热系数下导热效果的验证,以及不同厚度相同工况下绝缘性能差异的探究,选择更适合实际工况的导热硅胶垫。通过进一步验证PI膜对导热系数的影响,不同压力/压缩变形量下的热阻变化,以及导热系数随时间的变化情况,探究PI膜导热硅胶垫关键性能的变化,并为后续导热硅胶垫的选用提供理论依据和数据支持。     

Silicone insulators of power transmission lines with a variable inorganic load concentration: Electrical and physiochemical analyses

Polymeric insulation is an increasing tendency in projects and maintenance of electrical networks for power distribution and transmission. Electrical power devices (e.g., insulators and surge arresters) developed by using polymeric insulation presents many advantages compared to the prior power components using ceramic insulation, such as: a better performance under high pollution environment; high hydrophobicity; high resistance to mechanical, electrical and chemical stresses. The practice with silicone insulators in polluted environments has shown that the ideal performance is directly related to insulator design and polymer formulation. One of the most common misunderstandings in the design of silicone compounds for insulators is the amount of inorganic load used in their formulation. This paper attempts to clarify how the variation of the inorganic load amount affects physicochemical characteristics of different silicone compounds. The physicochemical evaluation is performed from several measurements, such as: density, hardness, elongation, tensile strength. In addition, the evaluation of the physicochemical structure is carried out using infrared test and scanning electronic microscopy (SEM). The electrical analysis is performed from the electric tracking wheel and erosion test, in agreement with the recommendation of the International Electrotechnical Commission (IEC).     

Tribological behaviour of epoxy based composites for rapid tooling

Epoxy resin composites are frequently applied in moulds manufactured with rapid tooling technologies that are used for wax and polymer materials injection. With the propose of enlarging the application field of the polymer matrix systems, it is fundamental to select adequate dispersed phases and analyse their influence on the composite properties in order to reinforce the polymer matrix and tailor the properties according to the tools specifications.Thermal conductivity and wear resistance are critical parameters for a good service performance and durability of the mould. Metallic fillers allow significant improvement in the resin thermal conductivity. In this work, it was possible to show that small amounts of milled fibres enhance the wear resistance, with little changes in the processability and in the allowed aluminium concentration in the resin matrix.A tribological study of these materials was performed involving the neat resin, the aluminium filled resin and tri-phase composites composed by epoxy, aluminium particles and milled glass or carbon fibres. The study was focused on the role of the particles and fibres in the friction and wear at room temperature and at a typical plastic injection temperature of 160 °C.     

Thermal analysis of high power LEDs on the MCPCB

The management of the reduced junction temperature of LEDs is a critical issue because it will affect many physical parameters such as light output, wave length and LED’s lifetime. The model used in this simulation consists of a metal core PCB attached with six chips(GaN on sapphire, Ag paste, cathode/anode, silicone encapsulant, mold frame) for 5W LED module. The MCPCB is composed of an aluminum base plate, a thin layer of dielectric, and a layer of copper. The temperature distribution of the developed LED module was simulated, and the thermal behavior within this 3-D model was investigated by using a commercial computational fluid dynamic code (Fluent 6.3). The results showed that the temperature variation along the vertical direction is more dominant than that in the circumferential direction due to the heat spreading effect of the copper layer. The ratio of heat dissipation through the each thermal path was calculated and compared for various input conditions. Several parameters that increase the junction temperature, such as the thermal conductivity and thickness of the dielectric layer and the encapsulate material, heat transfer coefficient and input power were also examined. Finally, a combination of designs for attenuating the junction temperature was proposed.     

气凝胶填充金属蜂窝夹层结构隔热性能试验与模拟

在1300℃温度和30 min保温时间的条件下,使用Nb基钎料对铌合金进行钎焊来成形铌合金蜂窝。对铌合金蜂窝与气凝胶填充铌合金蜂窝进行加热试验,测定了热面与冷面的瞬态温度。在与实际试验条件基本保持一致的情况下,建立了金属蜂窝与气凝胶填充金属蜂窝的有限元模型,并对不同几何参数的蜂窝进行传热模拟,分析了蜂窝芯格壁厚、芯体高度、芯格内径对隔热性能的影响,并以此总结出蜂窝的隔热机理。研究结果表明：气凝胶可有效地提高蜂窝隔热性能;芯格壁厚越小,芯体高度越大,蜂窝隔热性能越好;填充气凝胶时,芯格内径越大隔热性能越好,蜂窝芯空腔时,芯格内径越大,隔热性能越差。     

多组分纤维混杂增强树脂基摩擦材料研究

为提高摩擦材料高温下的摩擦磨损性能和摩擦因数的稳定性,利用正交试验法对多种纤维增强酚醛树脂基摩擦材料的配方进行优化设计,并通过极差分析,探讨多种纤维及含量对摩擦材料性能的影响及摩擦材料的磨损机制.研究表明:混杂纤维增强树脂基摩擦材料有着优异的耐磨性.陶瓷纤维硬度较高,开散混料后能够均匀分布在树脂基体内,对酚醛树脂基摩擦...     

Improvement of temperature accuracy in oil cooler systems with gas bypass

In keeping with the development of machine tools with higher speed, more axes, and a greater degree of sophistication, thermal deformation is becoming an important factor in the precision of machine tools. It has been found that thermal error accounts for about 70% of the total error in machine tools. As such, oil coolers which absorb heat from heat generating parts with cold oil are being used to reduce the error caused by thermal deformation. The gas bypass type oil coolers used in ultra-precision (temperature accuracy within ±0.1°C) machine tools are simple in structure and precise in terms of their temperature control performance; however, they have a limitation as regards temperature control due to the instability of their performance under light load conditions. In this study, an oil cooler system equipped with dual electronic valves was developed to solve the problems of the single electronic valve system and achieve more precise temperature control. To verify the performance of the developed system, its performance under the operating conditions of rated load, DIN 8602 standard, and ISO/DIS 230-3 operational mode was compared and analyzed. The proposed oil cooler system is applicable to semiconductor equipment, ultra-precision injection molds, and ultra-precision machine tools, and improves the quality of the products.     

固体火箭发动机抗烧蚀防热涂层的研究

直径及开口都较大的固体火箭发动机燃烧室大都采用橡胶基绝热层,但是,对于长细比大,或者是开口较小的客体,采用橡胶基绝热层在工艺上难以实现.为了寻找同时具备隔热效果良好,且针对小口径壳体工艺可行性高的内防热材料,我们开展了以环氧树脂、橡胶为基体,云母粉等耐高温无机填料组成的防热材料.通过试件测试及产品验证,证明该防热涂层也是固发燃烧室一种较为适宜的烧蚀防热材料,它不受被保护产品的几何形状限制,烧蚀率较小.     

Analysis of thermal conductivity in HI-LEDs lighting materials

The present study devised a measurement system to estimate the thermal conductivity of electronic product materials, especially in HILEDs lighting materials, exhibiting distinct thermal characteristics by conducting thermal performance experiments and theoretical analyses. First, steady-state conduction analysis with thermal resistance method was investigated on three composite material substrates of unknown heat conduction coefficients through a substrate material named Bakelite of low thermal conductivity revealing stable quality. Second, one-dimension semi-infinite transient conduction analysis was utilized to investigate metal materials with high thermal conductivities. Results showed that the Bakelite experimental module was verified for 62.5 % of the original wattages, which closest to the thermal conductivity 0.233 W/m-K of the Bakelite. And these composite materials M1, M2 and M3 composed of polymer and epoxy were 1.311, 0.844 and 2.403 W/m-K, respectively. The thermal performance experiments were investigated and the results have proved the correctness of the theoretical model. According to the experimental results, calculating the temperature value of the metal materials comprising cotton insulation and the transient analysis, this study determined the temperature error to be less 20 %. Consequently, a transient measurement system and method for metal materials with high heat conduction coefficients was established. Finally, the results of this work are the useful thermal conductivity method to facilitate rapid analysis in the future.

     

真空平板玻璃的性能及制造技术研究

真空平板玻璃是一种透明、节能型玻璃深加工产品,真空平板玻璃有优良保温隔热性能、防雾防露、隔音性能、抗风压性能、超长的耐久性。真空玻璃运用保温瓶的原理,放置两片平行的玻璃板四周封边而形成空间,并对该空间抽真空,从而使其形成真空层。真空平板玻璃的封接一般采用高温炉熔封接法,真空平板玻璃的支撑可以采用在支撑物的至少一个端面上涂低熔点金属或焊接玻璃,通过加热处理使支撑物固定在玻璃板上,以确保其位置。