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Vertically aligned carbon nanotube‐based composite: Elaboration and monitoring of the nanotubes alignment
Authors:Mickael Huard  Florent Roussel  Stéphan Rouzière  Stéphanie Patel  Mathieu Pinault  Martine Mayne‐L'Hermite  Pascale Launois
Affiliation:1. Laboratoire de Physique des Solides, UMR CNRS 8502, Université Paris Sud 11, Orsay Cedex, France;2. Laboratoire Francis Perrin ‐ CEA CNRS URA 2453, CEA Saclay, Gif‐sur‐Yvette Cedex, France
Abstract:We present the different elaboration steps of a composite formed of carbon nanotubes (CNT) carpet embedded in an epoxy polymer. Detailed characterization at each step of the elaboration process is performed. The good alignment of CNT in as‐grown carpets is kept all along the elaboration process of the composite, as it is measured at both macro and microscopic scales by X‐ray scattering. We also ensured by X‐ray fluorescence measurements that the iron‐based catalyst particles used for the synthesis were removed from the carpet after a high temperature post‐annealing treatment. These measurements give valuable information for further applications involving unidirectional nanotube composites and membranes, where CNT alignment is a key parameter. © 2013 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2014 , 131, 39730.
Keywords:composites  nanotubes  graphene and fullerenes  X‐ray  membranes  microscopy
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